Uranium Electrodeposition for Alpha Spectrometric Source Preparation
Natural uranium, Electrodeposition, Resolution, Uranium nitrates, Alpha spectrometry
Digital Object Identifier (DOI)
In this paper a simple method was used to design and set up an electrodeposition device for uranium source preparation for alpha spectrometry measurements. The aim of this work is to find the optimal parameters to be used to achieve uranium alpha sources with good spectral properties and maximum yield of the electrodeposition process. Samples with specific uranium activity were prepared from aqueous solution of uranyl nitrate hexahydrate (UO2 (NO3)2·6H2O). A series of preliminary experiments was conducted to establish the main parameters that have a significant influence on the deposition efficiency. Among these, the electrodeposition time was studied and the optimum time was found to be 1 h, in the case of our home-made deposition cell. It was also shown that a current of 1,500 mA, plating time of 60 min and pH range of 2–2.2 are the best conditions for deposition of uranium. The alpha spectrometry results show a good spectral resolution for the uranium sources obtained by the electrodeposition using the optimal parameters.
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Citation / Publisher Attribution
Journal of Radioanalytical and Nuclear Chemistry, v. 298, issue 2, p. 1335-1339
Scholar Commons Citation
Dumitru, Oana Alexandra; Begy, R. Cs.; Nita, D. C.; Bobos, L. D.; and Cosma, C., "Uranium Electrodeposition for Alpha Spectrometric Source Preparation" (2013). School of Geosciences Student Publications. 22.